SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.上海禹重实业有限公司为您提供分析仪,欢迎您的来电!CS230分析仪采购
力可ONH836氧氮氢分析仪特征稳固的炉头试样加载结构试样加载过程中完全密闭,消除大气的中可能带来的杂质的污染;简化日常分析所需的炉头进样部分机械维护工作。可选的自动功能上下电极自动清扫装置;20位试样及坩埚自动进样装置。附加功能及优点可选六轴可旋转触摸屏幕,增强了操作的工效和直观性;可选具有压力补偿和温度控制性能的标气检测气路;新型气路管道减少气路连接阀,使得漏气,断路故障更少;配置SmartLineRemote远程诊断功能。常熟分析仪价格分析仪,就选上海禹重实业有限公司,用户的信赖之选,有想法的不要错过哦!
SoftwareFeatures&BenefitsCornerstonebrandsoftwareisdividedintofourmainsections—Analysis,Diagnostics,Settings,andInstrument—forsimplifiednavigationandorganization.Toolbars,sliders,anddrop-downmenusmakeiteasytosetparametersforcalibrationanddataprocessing.Thesoftwarealsoincludesreal-timeambientmonitors,withfullyanimatedsystemdiagrams.Advanceddiagnosticfeaturesincludeathoroughdigitalon-boardmanual,maintenanceanimations,photoillustrations,"text-indent:25px">Procedure–Powder/ChipSamplesInstrumentcalibration/driftcorrection.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.PlacetheNickelCapsulecontainingthesampleintotheopenportatthetopoftheloadinghead.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodeeithermanuallyorremovethecrucibleandpresstheanalyzebuttontocleanwithanautomaticcleanerifapplicable.上海禹重实业有限公司是一家专业提供分析仪的公司,有想法的不要错过哦!
Procedure–Powder/ChipSamplesPreparetheinstrumentasoutlinedintheoperatorsinstructionmanual.Determinetheinstrumentblank.LoginaminimumofthreeBlankreps.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Inserta***NickelCapsule(leavecapsuleopen)intotheopenportattopofloadinghead.Note:samplesusingautomationshouldbeplacedintheappropriateautoloaderpositionbeforestartingtheanalysissequence.Oncethesequencehasstarted,theautomaticanalysiswillstartandendautomatically.分析仪,就选上海禹重实业有限公司,有需求可以来电咨询!盐城H836分析仪
上海禹重实业有限公司为您提供分析仪,欢迎新老客户来电!CS230分析仪采购
SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.CS230分析仪采购
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